114772-54-2

  • Product Name:2'-Cyano-4-Bromomethyl Biphenyl
  • Molecular Formula:C14H10BrN
  • Purity:99%
  • Molecular Weight:272.144
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Product Details;

CasNo: 114772-54-2

Molecular Formula: C14H10BrN

Appearance: Cream powder

Factory Supply Industrial Grade 2'-Cyano-4-Bromomethyl Biphenyl 114772-54-2 with Best Price

  • Molecular Formula:C14H10BrN
  • Molecular Weight:272.144
  • Appearance/Colour:Cream powder 
  • Vapor Pressure:0.1-0.2Pa at 20-25℃ 
  • Melting Point:125-128 °C(lit.) 
  • Boiling Point:413.2°Cat760mmHg 
  • Flash Point:203.7°C 
  • PSA:23.79000 
  • Density:1.43 g/cm3 
  • LogP:4.12018 

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114772-54-2 Process route

2-Cyano-4'-methylbiphenyl
114772-53-1

2-Cyano-4'-methylbiphenyl

2-(4,4-dibromomethylphenyl)benzonitrile
209911-63-7

2-(4,4-dibromomethylphenyl)benzonitrile

4'-(bromomethyl)-1,1'-biphenyl-2-carbonitrile
114772-54-2

4'-(bromomethyl)-1,1'-biphenyl-2-carbonitrile

Conditions
Conditions Yield
With N-Bromosuccinimide; Azo-bis(2,4-dimethyl-valeronitril); In dichloromethane; at 45 - 50 ℃; for 2 - 5h; Industry scale;
82%
With sodium bromate; hydrogen bromide; In dichloromethane; water; at 0 - 20 ℃; UV-irradiation;
80%
10%
With sodium bromate; azobis(2-cyanobutane); bromine; In water; chlorobenzene; at 70 - 80 ℃; for 6h;
69%
With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; cyclohexane; at 75 ℃; for 18h;
45%
17%
With sodium bromate; bromine; 2,2'-azobis(isobutyronitrile); In water; chlorobenzene; at 70 - 85 ℃; for 5h;
63.6 %Chromat.
36.2 %Chromat.
With sodium bromate; azobis(2-cyanobutane); bromine; In water; chlorobenzene; at 70 - 85 ℃; for 5h;
 
With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In dichloromethane; at 40 - 45 ℃; for 4 - 5h;
 
With N-Bromosuccinimide; In acetonitrile; Overall yield = 164 mg; Irradiation; Flow reactor;
 
2-cyano-4-methylbiphenyl
64113-85-5

2-cyano-4-methylbiphenyl

4'-(bromomethyl)-1,1'-biphenyl-2-carbonitrile
114772-54-2

4'-(bromomethyl)-1,1'-biphenyl-2-carbonitrile

Conditions
Conditions Yield
With 5,5-dibromohydantoin; In dichloromethane; at 50 ℃; for 0.5h; Temperature; Reagent/catalyst; Irradiation;
94%
With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; at 100 ℃; for 2h;
 

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